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Cyclohexene Essay Topics & Paper Examples

Preparation and Distillation of Cyclohexene

An experiment was carried out to synthesize cyclohexene by the dehydration of cyclohexanol using concentrated acid as a dehydrating catalyst. Subsequently the product was separated from the reaction mixture (solution instead) by distillation. Analytical techniques like Infrared Spectroscopy and Gas Chromatography were used for identifying and quantifying the different constituents in the reaction mixture. Procedure: The reaction was carried out by mixing 7. 3 ml of cyclohexanol and 1. 75 ml of 85 % H3PO4 in a 50 ml round bottom flask. An apparatus for dehydration of cyclohexanol was set up, with a fractionating column, a distillation adapter, a thermometer, a condenser, and a vacuum adapter. A rubber septum was used to provide a seal between the thermometer and the…